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Heteronuclear lanthanide‐based coordination polymers are microcrystalline powders, the luminescence properties of which can be precisely tuned by judicious choice of the rare‐earth ions. In this study, we demonstrate that such materials can also be obtained as stable solutions of nanoparticles in non‐toxic polyols. Bulk powders of the formula [Ln2−2xLn′2x(bdc)3⋅4 H2O]∞ (where H2bdc denotes 1,4‐benzene‐dicarboxylic...
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