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[Hg 6 P 4 ](TiCl 6 )Cl is synthesized in an ampoule at 400°C. Its crystal structure is solved on the basis of a CAD4 single-crystal experiment in a cubic space group Pa-3 (a=11.7675(6) Å, Z=4, R=0.0331). The structure is comprised of the three-dimensional cationic framework 3∞ [Hg 6 P 4 ] 4+ , and two different guest anions, octahedral TiCl...
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