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Grafting of [Mo(NAr)(CHCMe 2 R)(CH 2 tBu) 2 ], 1-R (R=Me or Ph) on the surface silanols of SiO 2-(700) gives 2-R through the electrophilic cleavage of the Mo–C σ-bond according to labelling (GC/MS and solid-state NMR) and reactivity studies (monitoring initiation). Similarly, molecular silanol derivatives react with 1-Ph also to give directly the monosiloxy derivatives...
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