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A single crystal of FeSb 2 about 5mm in diameter and 10mm in length with a tapering spire was grown by the gradient freeze technique combining the Bridgman technique and flux method using Sb-rich melts in sealed quartz ampoules. X-ray powder diffraction pattern of single crystal FeSb 2 indicates that it is a single phase marcasite structure. Clear Laue spots and scanning electron microscopy...
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