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2,5-Dimethylthiophene (2,5-Me 2 T) and Tp Me2 Ir(C 2 H 4 ) 2 react at 60 o C to give a mixture of two products, 3 and 4. Both derive from initial aromatic C H bond activation, but the organic ligand of 4 results from additional aliphatic C H cleavage and C C coupling of the activated C ar with a C 2 unit from the starting...
Five-coordinate complexes, [Ni(S 2 COR)(TRIPHOS)]X (R = cyclo-C 6 H 11 , X = Cl, PF 6 , [Ni(S 2 COC 6 H 11 ) 3 ]; R = Et, X = PF 6 , [Ni(S 2 COEt) 3 ]), have been obtained by the reaction of O-alkyldithiocarbonato complexes, [Ni(S 2 COR) 2 ], with bis(2-diphenylphosphinoethyl)phenylphosphine...
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