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The LnCl 3 /RLi reagent system commonly used with Ln=Ce for organic alkylation reactions has been studied with Ln=Y to make use of the 89 Y nucleus (I = 1/2) in NMR analyses. The ‘YCl’ obtained by the current literature methods of dehydrating LnCl 3 (H 2 O) x reagents in the LnCl 3 /RLi system contains water by elemental analysis, by reactivity with...
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