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We describe phase transitions in microfilm assemblies of octanethiol (OT)-capped 2–4nm-diameter Ag nanoclusters prepared from solutions with OT/Ag + ratios of ∼50. Using DSC we observe two melting/crystallization-type reversible phase transitions: one at ∼61°C due to interdigiated unattached octanethiol, and the other at ∼125°C due to the phase comprised of the assembly of OT-capped nanoclusters...
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