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Hierarchical organosilicate sorbents were synthesized which possess structure on two length scales: macropores of approximately 1μm lined by mesopores (35–45Å). The incorporation of macropores provides enhanced flow-through characteristics over purely mesoporous materials, thereby reducing back pressure when used in column formats. Materials of this type with varied surface groups were applied to...
Periodic mesoporous organosilicas (PMOs) with diethylbenzene bridging groups (DEB) in the pore walls are promising adsorbents for harmful compounds including nitroenergetics. The hierarchical macropore–mesopore structures developed here are expected to facilitate diffusion for such applications and to offer the potential for application in column formats. DEB-functionalized PMOs were synthesized with...
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