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A new series of shape‐persistent metallomacromolecules G0 and G1 as well as corresponding ligands, based on thiophene‐functionalized bisterpyridine‐Ru(II) with truxene moieties, as the nodes, were developed. All new compounds were fully characterized by 1H, COSY, and 13C NMR, as well as MALDI‐TOF MS. Their photophysical properties revealed that the branched scaffold resulted in high molar absorption...
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