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A [c2]daisy chain rotaxane with two diarylacetylene cores was efficiently synthesized in 53 % yield by capping a C2‐symmetric pseudo[2]rotaxane composed of two diarylacetylene‐substituted permethylated α‐cyclodextrins (PM α‐CDs) with aniline stoppers. The maximum absorption wavelength of the [c2]daisy chain rotaxane remained almost unchanged in various solvents, unlike that of the stoppered monomer,...
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