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In the present work, the high‐energy X‐ray diffraction (XRD) measurements performed using monochromatic synchrotron radiation of 112 keV (λ=0.110696 Å), were utilized to compare a phase constitution of melt‐spun ribbon and suction‐cast rods of Fe61Co10+xZr5W4–xB20 alloys (where x = 0, 2, 3 at.%). For bulk amorphous samples of the investigated alloys DSC studies allowed to determine the activation...
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