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A new hydrogelator based on L‐phenylalanine with a long hydrophobic chain and positively charged terminus was synthesized, and its gelation behavior in H2O was investigated. Polarized optical microscopy (POM), field emission scanning electron microscopy (FE‐SEM), and X‐ray diffraction (XRD) results indicate that the hydrogelator self‐assembles into fibres‐like aggregates which then lead to the formation...