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A shape memory and healable epoxy was prepared based on esterification between diglycidyl ether of bisphenol A and tricarballylic acid. The healing was achieved through transesterification at the fracture surface between two epoxy blocks in a confined space assisted by shape recovery force. The shape recovery of the compression programmed epoxy at elevated temperature tightly closed the gap between...
In this study, a new polymer artificial muscle based healing-on-demand composite was prepared and characterized. The composite consists of polymer artificial muscle made of commercial fishing line, thermoset host, and thermoplastic particle. Three-point bending damage to the beam sample can be healed even at a constrained boundary condition upon local heating, undergoing a close-then-heal procedure...
A particulate composite dispersed with thermoplastic particles and strain hardened short shape memory polymer fibers was prepared to evaluate its ability to repeatedly heal wide-opened cracks per the two-step close-then-heal (CTH) self-healing scheme. A two-step coating approach was used to enhance the shape fixity and workability of the cold-drawn programmed short polyurethane fibers. The relationship...
The past decade has witnessed remarkable advances in stimuli-responsive shape memory polymers (SMPs) with potential applications in biomedical devices, aerospace, textiles, civil engineering, bionics engineering, energy, electronic engineering, and household products. Shape memory polymer composites (SMPCs) have further enhanced and broadened the applications of shape memory polymers. In addition...
Recently, shape memory polymer fibers (SMPFs) have been used in a biomimetic two-step (Close-Then-Heal) self-healing system for healing macroscopic cracks. The objective of this study was to investigate the effect of cold-drawing programming of SMPFs on the healing efficiency of conventional thermosetting polymer composites and the possibility of healing wide-opened crack by localized heating. To...
Cyclic stress-strain responses of a shape memory polymer based syntactic foam and pure SMP were investigated after a two dimensional (2-D) programming process. Three types of cyclic loading patterns were used: multiple compression-tension cycles at 5% maximum strain, one compression-tension cycle at 40% maximum strain, and one coupled thermo-mechanical cycle at 40% maximum strain. The results indicate...
In a previous study, a biomimic two-step self-healing scheme (close-then-heal (CTH)) by mimicking human skin has been proposed for self-healing structural-length scale damage [Li and Uppu. Composites Science and Technology 2010; 70: 1419–1427]. The purpose of this study is to validate this idea by fabricating a composite with thermoplastic particles (Copolyster) dispersed in a shape memory polymer...
While the current self-healing approaches such as micro-capsules, hollow fibers, thermally reversible covalent bonds, ionomers, incorporation of thermoplastic particles, etc., are very effective in self-healing micro-length scale damage, self-healing of structural scale or macro-length scale damage remains one of the grand challenges facing the self-healing community. We believe that self-healing...
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