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Highly ordered TiO 2 nanotube arrays were successfully prepared by electrochemical anodization in a formamide-based electrolyte containing 0.5wt.% NH 4 F and 2vol.% H 2 O. The effects of the calcining temperature, the calcining time and the heating rate on the formation of the TiO 2 nanotube arrays were investigated in detail. The morphological changes and phase transformations...
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