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A new intermetallic in the Ca-Au phase field has been synthesised, using an unusual high-pressure route, with the stoichiometry Ca 3 Au 4 . The structure of the intermetallic was investigated using powder X-ray and powder neutron diffraction techniques. Ca 3 Au 4 adopts the Pu 3 Pd 4 structure type, which crystallises in the rhombohedral space group...
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