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In situ high-energy X-ray diffraction was carried out to investigate the structural transformation of lithium cobalt oxides during the solid-state synthesis. Two allotropic phases were observed during the synthesis process; Li2Co2O4 with a spinel structure was formed within the temperature window between 450 °C and 650 °C, beyond which Li2Co2O4 was converted to its hexagonal counterpart, layered LiCoO...
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