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CeNiAl absorbs up to 1.93(5) hydrogen per formula unit at room temperature and at a pressure of 1 MPa. This hydride is stable in air. Hydrogenation induces both: (i) a structural transition hexagonal ZrNiAl-type→hexagonal AlB 2 -type; (ii) a valence transition for cerium. At low temperature for T<7 K, the hydride CeNiAlH 1.93 shows a spin fluctuation behaviour.
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