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The grafting reaction between a trifunctional silylating agent and two kinds of 2:1 type layered silicates was studied using FTIR, XRD, TGA, and 29 Si CP/MAS NMR. XRD patterns clearly indicate the introduction of 3-aminopropyltriethoxysilane (γ-APS) into the clay interlayer. In the natural montmorillonite, γ-APS adopts a parallel-bilayer arrangement, while it adopts a parallel-monolayer arrangement...
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