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A bismuth‐film electrode was employed to quantify Cd(II) and Zn(II) in estuarine water samples by anodic stripping voltammetry. The bismuth film was deposited in situ simultaneously with the analytes onto a carbon fibre disc microelectrode (radius=3 µm). Under the optimised conditions, calibration plots for both metallic ions were obtained in the range from 0.5 to 10.0 nmol L−1 and the limits of detection...
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