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XRD-pure Li4Mn5O12 spinels are obtained below 600 °C from oxalate and acetate precursors. The morphology consists of nanometric particles (about 25 nm) with a narrow particle size distribution. HRTEM and electron paramagnetic resonance (EPR) spectroscopy of Mn4+ are employed for local structure analysis. The HRTEM images recorded on nano-domains in Li4Mn5O12 reveal its complex structure. HRTEM shows...
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