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Methanol-to-olefin (MTO) conversion on microporous silico-aluminophosphates is particularly well-suited for the application of molecular-level concepts to the development of well-defined supported catalysts. The active site of a typical MTO catalyst is a nm-size inorganic cage with an essential organic component. Opportunities for altering the selectivity of such catalysts include tailoring the organic...
In situ NMR has been extensively applied in the past decade to obtain basic mechanistic information about reactions in heterogeneous catalysis. Most studies in the literature have employed either sealed glass ampoules of catalyst and adsorbate that are heated outside of the NMR probe or variable temperature studies of samples sealed in magic‐angle spinning (MAS) rotors. In situ NMR studies of sealed...
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