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Synchrotron X-ray reflectivity is used to study ion distributions at the liquid–liquid interface between a nitrobenzene solution of tetrabutylammonium tetraphenylborate (TBATPB) and a water solution of tetrabutylammonium bromide (TBABr). The concentration of TBABr is varied to alter the ion distribution. Our X-ray measurements are inconsistent with several commonly used theories of ion distributions,...
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