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In situ studies of acetylene oxidation on Pt(111) have been performed with both fluorescence yield near-edge spectroscopy (FYNES) and temperature-programmed FYNES (TP-FYNES) for temperatures up to 600 K and flowing oxygen pressures up to 0.009 Torr. Low-temperature spectroscopic (FYNES) results indicate that at 150 K acetylene adsorbs with the CC backbone tilted slightly up from the Pt(111) surface,...
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