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The double functionalization of styrenes through Cu‐mediated assisted tandem catalysis was developed. The reaction was initiated by Cu‐catalyzed aziridination and the subsequent nucleophilic ring‐opening, which was triggered by the addition of (NH4)2S2O8 as an oxidant of Cu‐catalyst to form a variety of C–C and C–X bonds. The expansion to three contiguous catalytic cycles led to the synthesis of functionalized...
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