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In this study, we present a simple process to obtain highly dispersed palladium nanoparticles on Vulcan XC-72R carbon support without any protective agent. To obtain high metal loading Pd/C catalyst without any surfactant, we modified the polyol process by employing NH 3 species as a mediation to control the reaction pathway to avoid the precipitation of Pd(OH) 2 , and hence the agglomeration...
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