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A series of hypercoordinated monoorganotin dibromides formed by glycolic acid amides, [RSnBr2(OCH2C(O)NR′2)]2 (2a, R=Et, NR′2=NMe2; 3a, R=n-Bu, NR′2=NMe2; 4b, R=Ph, NR′2=morpholin-4-yl), were obtained and investigated by X-ray analysis, multinuclear NMR spectroscopy in solutions (1H, 13C, 119Sn) and solid state (CP/MAS). It has been established that 2a, 3a and 4b in solid state are dimeric. For the...
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