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The four 18‐tungsto‐2‐arsenates(III) [MII(H2O)(TiIVO)2(α‐AsIIIW9O33)2]12– [M = Co (CoTi2), Ni (NiTi2), Cu (CuTi2), Zn (ZnTi2)] were rationally synthesized by treating the respective divalent metal ions with the monolacunary, dititanium(IV)‐containing polyanion precursor [(TiIVO)2(α‐AsIIIW9O33)2]14– (Ti2) in aqueous solution. All four polyanions are isostructural and correspond to dimers with two Ti...
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