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The black rubidium oxide Rb 4 O 6 has been described to be a mixed peroxide-hyperoxide Rb 4 (O 2-2 )(O -2 ) 2 in the literature. Previous X-ray diffraction studies on powders and single crystals, however, revealed that Rb 4 O 6 crystallises like cubic Pu 2 C 3 (space group 13d), and has only one crystallographically...
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