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Treatment under H 2 at 300 °C of Ru(COD)(COT) dispersed on silica yields 2 nm ruthenium nanoparticles, [Ru p /SiO 2 ], according to EXAFS, HRTEM and XPS. H 2 adsorption measurements on [Ru p /SiO 2 ] in the absence of O 2 show that Ru particles adsorb up to ca. 2H per surface ruthenium atoms (2H/Ru s ) on various samples; this technique...
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