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Reversible voltammetry of the anionic rubredoxin and ferredoxin proteins at a pyrolytic graphite edge plane electrode can be observed either by ex situ modification of the electrode with multivalent cations (poly(l-lysine), Cr(III) complexes) or by addition of these cations to the solution. However, poly(l-lysine) binds irreversibly to pyrolytic graphite and voltammograms obtained at an ex situ form...
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