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We have synthesized by solution methods and fully characterizedtwo sets of terminally protected peptides based on the tricyclic Cαα-disubstituted glycine Afc. Theconformational preferences of the Afc/Gly peptides were examined by FT-IR absorption and 1H NMR techniques, whilethose of the Afc/TOAC peptides were primarily investigated by using fluorescence spectroscopy. The X-ray diffraction structure...
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