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The title complex, [Mn 3 O(C 6 H 5 COO) 6 (py) 3 ] · 2CH 3 CN (py = pyridine), has been prepared. Single-crystal X-ray analysis revealed a μ 3 -oxo-bridged Mn 2III Mn II structure, in which each manganese atom has a distorted octahedral environment. The Mn(1) atom is readily assigned as a Mn III centre from the Mn-(μ...
A new mixed-valence heterotrinuclear complex [Mn III Co III Mn II O(PhCOO) 6 Py 3 ] was first synthesized by using NBu 4 MnO 4 as the oxidizer. In the reaction, Co II ions were oxidized to Co III , while Mn VII were reduced to Mn II and Mn II ...
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