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Nichtlineare optische Materialien In der Zuschrift auf S. 6598 beschreiben K. Ok, G. Zou et al. die Synthese des Fluoridsulfats CsSbF2SO4 aus KTiOPO4 durch chemische Substitution. CsSbF2SO4 zeichnet sich durch eine ausgeprägte Frequenzverdopplung aus.
A novel noncentrosymmetric (NCS) polar fluoride sulfate, CsSbF2SO4, was obtained by ionothermal synthesis. A meticulously designed co‐substitution approach was used to successfully replace the [TiO6]8− and [PO4]3− functional groups in KTiOPO4 (KTP) with [SbO4F2]7− and [SO4]2− units, respectively. The structure of CsSbF2SO4 features a pseudo‐3D framework consisting of interconnected 1D [SbF2O2SO4]5−...
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