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The new tris(perfluoroalkyl)borane carbonyls, (C2F5)3BCO and (C3F7)3BCO, were prepared by means of a novel synthetic route using commercially available precursors by reacting K[(C2F5)3BCOOH] and K[(C3F7)3BCOOH] with concentrated sulfuric acid in the last step. The carboxylic acids, K[(C2F5)3BCOOH] and K[(C3F7)3BCOOH], were prepared by oxidative cleavage of the CC triple bonds in Cs[(C2F5)3BCCPh]...
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