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The temperature dependence of crystal structure parameters of isostructural coordination polymers Fe2MO(Piv)6(bipy)1.5·2DMF [1·2DMF and 2·2DMF, where M = NiII or CoII, respectively, Piv = (CH3)3CCO2–, bipy = 4,4‐bipyridine and DMF is N,N‐dimethylformamide] was studied at five temperatures in the range from 120 to 296 K. The X‐ray structure of the N,N‐diethylformamide (DEF) solvate of the same coordination...
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