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The use of carboxylates in the synthesis of 3d/4f clusters, with or without a second organic ligand, has afforded a series of tetranuclear M 2 Gd 2 complexes (M=Fe or Mn), and two new trinuclear M 2 Gd (M=Fe or Mn) molecular compounds. Only one of these, [Mn 2 Gd 2 O 2 (O 2 CBu t ) 8 (HO 2 CBu t ) 4 ] (1),...
The use of a convenient source of Mn III ions, namely the [Mn(OR)(O 2 CR′) 2 ] n (R=H, Me, and R′=Me, Bu t ) family of 1-D coordination polymers, afforded two new enneanuclear and decanuclear molecular clusters, homometallic [Mn 9 O 7 (O 2 CBu t ) 13 (MeCN) 2 ] (3) and heterometallic [Mn 10−x Fe ...
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