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Nickel hydride (NiH) catalyzed hydrocarbonation has emerged as an efficient approach to construct new C−C bonds containing at least one C(sp3) center. However, the regioselectivity of this reaction is by far dictated by substrates. Described here is a strategy to achieve two different regioselectivites of hydroalkylation of the same substrates by using ligand control. This strategy enables the first...
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