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Photodecomposition of NH3 to H2 and N2 was carried out using metal-supported TiO2 (M/TiO2) photocatalysts in an aqueous NH3 solution under UV irradiation at room temperature. Ni/TiO2 photocatalysts indicated the highest yield of H2. The NH2 radical was formed as a dominant intermediate during NH3 decomposition, as confirmed by electron spin resonance measurements. Reaction pathways via NH2 radical...
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