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The tetramethylammonium salts (NMe 4 ) 2 [MO 2 (2,3-Hdhb) 2 ]·2H 2 O and (NMe 4 ) 2 [MO 2 (3,4-Hdhb) 2 ]·6H 2 O (M=Mo, W; Hdhb=monoprotonated form of 2,3- or 3,4-dihydroxybenzoic acid, 2,3-H 3 dhb or 3,4-H 3 dhb) were prepared and their crystal structures determined. The structure of [Mg(H 2 O)...
The tetrahexylammonium (THA) salt of the peroxocomplex [W 2 O 3 (O 2 ) 4 ] 2− was used as catalyst for the oxidation of cis-cyclooctene, geraniol and cyclooctane, with hydrogen peroxide, in acetonitrile. High catalytic activity for all substrates, with high efficiency of use of hydrogen peroxide, was found. Under the conditions used, the oxidation of cyclooctane...
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