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Different synthetic routes have been developed to obtain the aqua complex trans‐[RuII(trpy)(pypz‐H)(OH2)](PF6)2, Ru6. This complex, together with the chlorido intermediate complexes cis‐ and trans‐[RuIICl(pypz‐H)(trpy)]+, Ru5a and Ru5b, have been fully characterized by analytical, spectroscopic, and electrochemical methods. Furthermore, the trans‐Ru5b complex has been characterized in the solid state...
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