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The reaction between norbornene (C 7 H 10 ) and Ir 6 (CO) 16 in refluxing toluene yields the substituted cluster [Ir 6 (CO) 14 (C 7 H 8 )]. In the solid state, the six iridium atoms define an octahedral metal cage, and one face is capped by the C 7 H 8 ligand, coordinated through a 1,2-vinylidene unit. The loss of two...
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