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A trianionic ligand H3L [2‐hydroxy‐N‐(2‐{[(2‐hydroxyphenyl)methylene]amino}‐2‐methylpropyl)benzamide] with an inner N2O2 coordination site and an oxygen atom coming from an amide function not involved in this site yields a monoanionic LCo‐pipH+ complex, in which the CoII ion is in a square‐planar environment and a low‐spin state S = 1/2. Further reaction with GdCl3·6H2O and tetramethylheptanedione...
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