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A new organometallic cluster [Pt4(μ2-dpam)3(μ2-CO)3(η1-dpam)] X2 (X=CF3CO 2- ; 4a) was prepared from a reaction between Pt(dpam)(CF3CO2)2 and CO in a methanol (water mixture). The PF 6- salt 4b is obtained from an anion exchange with NH4PF6 in methanol. Dark red crystals suitable for X-ray crystallography (X=PF 6- ) revealed the commonly encountered butterfly structure for a 58-electron Pt cluster...
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