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By reacting Ru(CO)5 with the stoichiometric amount of Pt(C7H10)3(C7H10=bicyclo[2.2.1]heptene) in heptane and by removing the excess of CO, two polymorphs of Ru4Pt2(CO)18, 1, were isolated and characterized by X-ray diffraction, namely the already known monoclinic (α) and a new orthorhombic (β) phase. Crystal data of the β phase: space group Pna21; a=17.738(3), b=15.596(2), c=10.357(1), V=2865 Å3....
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