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Cyclic voltammetry (CV) of [Ru(phen)3]2+ (phen=1,10-phenanthroline) is studied in CH3CN under N2 at a gold electrode whose surface is modified by thiocyanate. Five one-electron ligand reductions are observed on the negative side of normal hydrogen electrode (NHE), which is unprecedented. Using Randles-Sevcik equation, the electrochemical radius of the electrode has been estimated as 0.86mm (cf. physical...
A dimeric double oximato-bridged (μ1,2-N-O) Cu(II) complex, [Cu2L2(ClO4)2]·2H2O (1), was synthesized from the reaction of equimolar proportion of a novel Schiff base ligand, 1-phenyl-1-(pyridin-2-yl-hydrazono)-propan-2-one oxime (LH), and copper(II)perchlorate hexahydrate in methanol. C, H and N microanalyses, gravimetric copper estimation, FT-IR, UV–Vis (solid state as well as in solution), ESI-MS...
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