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Pair distribution function analysis of in situ total scattering data recorded during formation of WO3 nanocrystals under hydrothermal conditions reveal that a complex precursor structure exists in solution. The WO6 polyhedra of the precursor cluster undergo reorientation before forming the nanocrystal. This reorientation is the critical element in the formation of different hexagonal polymporphs of...
Aluminiumoxid im Fluss: Auf Informationen aus Synchrotron‐Röntgenpulverbeugungs(PXRD)‐Messungen in situ, die einen Reaktionsmechanismus ohne kristalline Intermediate nahelegen, baut die erste einstufige und schnelle Synthese von γ‐Al2O3 im Großmaßstab auf. Das γ‐Al2O3 wurde bei niedriger Temperatur in einem kontinuierlichen Flussreaktor aus Aluminiumisopropoxid in 2‐Propanol/Wasser ohne anschließende...
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