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An amphiphile based on polyethylene glycol (PEG) polymer and two molecular moieties (perylene diimide and C7 fluoroalkyl, PDI and C7F) attached to its termini assembles into crystalline films with long‐range order. The films reversibly switch from crystalline to amorphous above the PEG melting temperature. The adaptive behavior stems from the responsiveness of the PEG domain and the robustness of...
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