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The self‐assembly of 3D colloidal supercrystals built from faceted 20 nm Bi nanocrystals is studied by in situ synchrotron X‐ray scattering combined with Monte Carlo simulations. The assembly is driven by nonsolvent into solvent diffusion. In article number 1802078, Rainer T. Lechner and co‐workers reveal a unique orientation phase: the nanocrystals' shape induces 6 distinct global orientations within...
When nanocrystals self assemble into ordered superstructures they form functional solids that may inherit the electronical properties of the single nanocrystals. To what extent these properties are enhanced depends on the positional and orientational order of the nanocrystals within the superstructure. Here, the formation of micrometer‐sized free‐standing supercrystals of faceted 20 nm Bi nanocrystals...
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