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Two positron emission tomography radiotracers for the glycine transporter 1 (GlyT1) are reported here. Each radiotracer is a propylsulfonamide‐containing benzamide and was labeled with either carbon‐11 or fluorine‐18. [11C]CMPyPB was synthesized by the alkylation of a 3‐hydroxypyridine precursor using [11C]MeI, and [18F]MK‐6577 was synthesized by a nucleophilic aromatic substitution reaction using...
Conversion of aldehydes and ketones to 1,3-dioxanes with 2-trimethylsilyl-1,3-propanediol affords carbonyl-protected products, ultimately susceptible to unmasking with LiBF 4 in THF.
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