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Synchrotron small angle X-ray scattering (SAXS) was performed to investigate the effect of dissolved CO2 in toluene on the conformation of polystyrene (PS) in the solution. It has been found that the second virial coefficientA2 and the radius of gyrationRg decrease with the increasing antisolvent CO2 pressure. The scattering intensity of PS chain followedI(h) ∞h−α under different antisolvent pressures...
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